Tolylboronic acid → HCID 86595318, compound

HRID 1009717Notes

Reaction equation

HRID 1009717 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([C:8]#[C:9][C:10]2[N:11]=[C:12]([CH3:15])[NH:13][CH:14]=2)[CH:5]=[CH:4][N:3]=1.[CH3:16][C:17]1[CH:22]=[CH:21][C:20](B(O)O)=[CH:19][CH:18]=1>>[Cl:1][C:2]1[CH:7]=[C:6]([C:8]#[C:9][C:10]2[N:11]=[C:12]([CH3:15])[N:13]([C:20]3[CH:21]=[CH:22][C:17]([CH3:16])=[CH:18][CH:19]=3)[CH:14]=2)[CH:5]=[CH:4][N:3]=1

Participants

3

Reactant 2

HCID 79799Tolylboronic acidHCID 178418879HCID 178418879, compound

Product 1

HCID 86595318HCID 86595318, compound

Procedure

The title compound, MS: m/e=308.8 (M+H+), was prepared in accordance with the general method of example 7 from 2-chloro-4-(2-methyl-1H-imidazol-4-ylethynyl)-pyridine and 4-methyl-benzene boronic acid.

Sources & evidence

ORD record
ord-4649426b92ef4c23a9f20db78e8dfd3d
Source dataset
uspto-grants-2011_07
Patent number
US07973165B2

Reaction notes

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