Naphthalene → HCID 86631015, compound

Participants

Reaction Steps

A mixture of lithium (12 mg, 1.73 mmol) and naphthalene (222 mg, 1.73 mmol) was stirred in THF (2.5 mL) at room temperature for 4 hours. As a result, a lithium-naphthalenide solution was prepared. To the solution, a solution in which Intermediate (VI) (130 mg, 0.41 mmol) was mixed with THF (1 mL) was added at room temperature. Immediately after the reaction mixture had been stirred for 5 minutes, the reaction mixture was mixed with a saturated ammonium chloride solution.

Provenance & Evidence