HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 67305374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Triacetoxyperiodinane | HCID 159087 | — |
| Reactant | 5-Hydroxy-2-(3-phenyl-pyrrolidine-1-carbonyl)-cyclohexanecarboxylic Acid Benzyl Ester | HCID 67305073 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67305374 | HCID 67305374 | — |
Reaction Steps
To a solution of alcohol compound from Step 2 (400 mg) was added Dess-Martin reagent (500 mg) and the mixture was stirred at rt for 3 h. After the reaction was complete the mixture was diluted with methylene chloride followed by the addition of 0.1 N NaOH aqueous solution
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07973041B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-4ed0aa19b60a4004b0f251a8ade3f6fe |
| Source note | uspto-grants-2011_07 |