Methyl Acetate → HCID 67021552, compound

HRID 1010719Notes

Reaction equation

HRID 1010719 reaction equation
[CH3:1][O:2][C:3](=[O:19])[CH2:4][C:5]1[CH:10]=[CH:9][C:8]([NH:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=2[NH2:18])=[CH:7][CH:6]=1.[CH3:20]OC(=O)C>>[CH3:1][O:2][C:3](=[O:19])[CH2:4][C:5]1[CH:6]=[CH:7][C:8]([N:11]2[C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=3[N:18]=[CH:20]2)=[CH:9][CH:10]=1

Participants

3

Reactant 2

HCID 6584Methyl AcetateHCID 67021316HCID 67021316, compound

Product 1

HCID 67021552HCID 67021552, compound

Procedure

is obtained analogously to the method as described in Step 1.2 but using [4-(2-amino-phenylamino)-phenyl]-acetic acid methyl ester instead of 4-(3-amino-pyridin-2-ylamino)-phenyl]-acetic acid methyl ester as a starting material. ES-MS: 267.1 [M+H]+; single peak at tR=3.00 min (System 1).

Workup

  1. customis obtained analogously to the method

Sources & evidence

ORD record
ord-baf0808ff85d430f8c3851d58b9995a8
Source dataset
uspto-grants-2011_07
Patent number
US07977338B2

Reaction notes

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