HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Ethanediamine, N1,N1-diethyl-N2-methyl- → HCID 58478813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Ethanediamine, N1,N1-diethyl-N2-methyl- | HCID 66034 | — |
| Reactant | HCID 58478730 | HCID 58478730 | — |
| Product | HCID 58478813 | HCID 58478813 | 76% |
Reaction Steps
In a process similar to that described in Preparation 8, 3-(5-Oxo-5,7-dihydro-furo[3,4-b]pyridin-2-yl)-propionaldehyde (61 mg, 0.32 mmol) and N,N-diethyl-N′-methylethylenediamine (33 μL, 0.32 mmol) are reacted to provide the title compound as white solid (60 mg, 76%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977351B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-39a9fe4ca7d64f58aeb69289a667f69f |
| Source note | uspto-grants-2011_07 |