1-Bromohexane → 1-Ethynyl-2-n-octadecylnaphthalene

HRID 1011845Notes

Reaction equation

HRID 1011845 reaction equation
[C:1]([C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][C:4]=1[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])#[CH:2].BrCCCCCC.Br[CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38]CCCCCC>>[C:1]([C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][C:4]=1[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:38][CH2:37][CH2:36][CH2:35][CH2:34][CH2:33][CH2:32][CH2:31][CH2:30][CH2:29][CH2:28][CH3:27])#[CH:2]

Participants

4

Reactant 3

HCID 81011-BromohexaneHCID 82181-BromooctadecaneHCID 21954826HCID 21954826, compound

Product 1

HCID 866289541-Ethynyl-2-n-octadecylnaphthalene

Procedure

1-Ethynyl-2-n-octadecylnaphthalene was prepared in a similar manner to 1-ethynyl-2-hexylnaphthalene, except that bromohexane was replaced by bromo-n-octadecane.

Sources & evidence

ORD record
ord-94aac1a2fbdb45538a19f4ff3e28b2d2
Source dataset
uspto-grants-2011_07
Patent number
US07977441B2

Reaction notes

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