HuagongsheHuagongshe Chemistry Print Report · For research reference only
TIBA isododecane → 2,3,5-Triiodobenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | TIBA isododecane | HCID 131728349 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2,3,5-Triiodobenzoic acid | HCID 6948 | — |
Reaction Steps
9.8 cc of TIBA/isododecane solution (101 g/L) were mixed with 1.91 cc of MAO/toluene solution (Albemarle -30% wt) to obtain a MAO/TIBA molar ratio of 2:1. The solution was stirred for 1 hour at room temperature. Then, 26 mg of A-1 were dissolved in the solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977444B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-b1c79844f75f48d4949d31fdccf96742 |
| Source note | uspto-grants-2011_07 |