Benzene, 1-iodo-3-(trifluoromethyl)- → HCID 67314648, compound

HRID 1011879Notes

Reaction equation

HRID 1011879 reaction equation
[CH3:1][O:2][C:3]([C:5]1[C:6]([CH:13]2[CH2:15][CH2:14]2)=[N:7][NH:8][C:9]=1[CH:10]1[CH2:12][CH2:11]1)=[O:4].[F:16][C:17]([F:26])([F:25])[C:18]1[CH:19]=[C:20](I)[CH:21]=[CH:22][CH:23]=1>>[CH3:1][O:2][C:3]([C:5]1[C:6]([CH:13]2[CH2:15][CH2:14]2)=[N:7][N:8]([C:22]2[CH:21]=[CH:20][CH:19]=[C:18]([C:17]([F:26])([F:25])[F:16])[CH:23]=2)[C:9]=1[CH:10]1[CH2:12][CH2:11]1)=[O:4]

Participants

3

Reactant 2

HCID 67868Benzene, 1-iodo-3-(trifluoromethyl)-HCID 67314850HCID 67314850, compound

Product 1

HCID 67314648HCID 67314648, compound

Procedure

The title compound was prepared by reaction of intermediate 16B 3,5-dicyclopropyl-1H-pyrazole-4-carboxylic acid methyl ester with 3-trifluoromethlyiodobenzene in analogy to intermediate 6A. MS: 367.2 (MH+).

Sources & evidence

ORD record
ord-1908e9c23541441aac4ad881cb6a7a47
Source dataset
uspto-grants-2011_07
Patent number
US07977358B2

Reaction notes

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