HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetoacetate → Rac-2-acetyl-4-methoxy-3-oxo-butyric acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | Methoxyacetyl chloride | HCID 96623 | — |
| Product | Rac-2-acetyl-4-methoxy-3-oxo-butyric acid ethyl ester | HCID 87352689 | — |
Reaction Steps
In analogy to the procedure described in Intermediate 11A], ethyl acetoacetate and methoxyacetylchloride gave the crude title compound in quantitative yield as yellow oil. MS: 202.9 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977358B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-525af10a5d2c4ad5b29c769a55edaab5 |
| Source note | uspto-grants-2011_07 |