HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrimidine-5-carboxaldehyde → N-[(E)-pyrimidin-5-ylmethylideneamino]-3-(trifluoromethoxy)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrimidine-5-carboxaldehyde | HCID 2761034 | — |
| Reactant | [3-(Trifluoromethoxy)phenyl]hydrazine | HCID 5194226 | — |
| Product | N-[(E)-pyrimidin-5-ylmethylideneamino]-3-(trifluoromethoxy)aniline | HCID 87352512 | 12% |
Reaction Steps
In analogy to the procedure described in Example 167A], pyrimidine-5-carbaldehyde and (3-trifluoromethoxy-phenyl)-hydrazine gave the title compound as an orange solid (12%). MS: 281.5 (M−H−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977358B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-b57ab6bc8ebd4a918a636321e067471f |
| Source note | uspto-grants-2011_07 |