(3-(Trifluoromethyl)phenyl)hydrazine → HCID 87352854, compound

HRID 1011989Notes

Reaction equation

HRID 1011989 reaction equation
[F:1][C:2]([F:12])([F:11])[C:3]1[CH:4]=[C:5]([NH:9][NH2:10])[CH:6]=[CH:7][CH:8]=1.[N:13]1[CH:18]=[C:17]([CH:19]=O)[CH:16]=[N:15][CH:14]=1>>[N:13]1[CH:18]=[C:17](/[CH:19]=[N:10]/[NH:9][C:5]2[CH:6]=[CH:7][CH:8]=[C:3]([C:2]([F:11])([F:12])[F:1])[CH:4]=2)[CH:16]=[N:15][CH:14]=1

Participants

3

Reactant 2

HCID 98650(3-(Trifluoromethyl)phenyl)hydrazineHCID 2761034Pyrimidine-5-carboxaldehyde

Product 1

HCID 87352854HCID 87352854, compoundYield 87%

Procedure

In analogy to the procedure described in Example 167A], 3-(trifluoromethyl)phenylhydrazine and pyrimidine-5-carbaldehyde gave the title compound as a yellow solid (87%). MS: 267.1 (MH+).

Sources & evidence

ORD record
ord-b7f4dd5b95bc4531bdafe2798f78a331
Source dataset
uspto-grants-2011_07
Patent number
US07977358B2

Reaction notes

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