HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1012172Generated: October 30, 2026
Dimethylformamide dimethyl acetal → HCID 67313456, compound
https://huagongshe.com/reaction/1012172
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 5-Acetylthiophene-2-carboxylic acid | HCID 3742727 | — |
| Product | HCID 67313456 | HCID 67313456 | — |
Reaction Steps
5-Acetyl-thiophene-2-carboxylic acid (1 g, 5.87 mmol) was treated with N,N-dimethylformamide dimethylacetal (10 mL) and heated at 120° C. for 16 hours. The mixture was dried in vacuo to give 5-(3-dimethylamino-acryloyl)thiophene-2-carboxylic acid which was taken to the next step. MS: m/z 226 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07977481B2 |
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| Source dataset | uspto-grants-2011_07 |
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| ORD ID | ord-40ed0d6f6b4a4d31a3d57d79fa9c4be8 |
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| Source note | uspto-grants-2011_07 |
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