Methyl iodide → HCID 86624032, compound

Participants

Reaction Steps

Into 20 mL of chloroform was dissolved 10 g of 2-(4-(2,2-bis(4-(6-(4-(cyanophenyl)phenoxy)hexyloxy)phenylthio)ethoxy)phenylthio)pyridine, and then 10 mL of methyl iodide was added thereto. The resultant solution was then heated under reflux. After the completion of the reaction, the solvent and an excess amount of methyl iodide were removed by distillation under reduced pressure. The residue was dissolved in chloroform, and purified by silica gel column chromatography (yielded amount 7.5 g, and yield 65.9%).

Provenance & Evidence