Propionic Acid → Palladium(II) propionate

HRID 1012890Notes

Reaction equation

HRID 1012890 reaction equation
CC(O)=O.CC(O)=O.[Pd:9].[C:10]([OH:14])(=[O:13])[CH2:11][CH3:12]>>[C:10]([O-:14])(=[O:13])[CH2:11][CH3:12].[Pd+2:9].[C:10]([O-:14])(=[O:13])[CH2:11][CH3:12]

Participants

3

Reactant 2

HCID 1032Propionic AcidHCID 4144353Palladium (II) acetate

Product 1

HCID 11459426Palladium(II) propionate

Procedure

5 gm commercial palladium(II) acetate trimer (Aldrich) was added to 40 g of propionic acid. The mixture was maintained at 40 degrees Celsius for 24 hours. Excess propionic acid was removed under vacuum at room temperature. The resulting yellow solid was used for making palladium inks.

Workup

  1. temperatureThe mixture was maintained at 40 degrees Celsius for 24 hours
  2. customExcess propionic acid was removed under vacuum at room temperature

Sources & evidence

ORD record
ord-3e12e740c6eb4a24a7d78bb4c1efa40f
Source dataset
uspto-grants-2011_07
Patent number
US07981508B1

Reaction notes

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