HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzo(B)Thiophene → HCID 178516913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzo(B)Thiophene | HCID 7221 | — |
| Reactant | 3-Oxo-3,4-dihydro-2H-1,4-benzothiazine-6-carbaldehyde | HCID 10943348 | — |
| Reactant | HCID 178502731 | HCID 178502731 | — |
| Product | HCID 178516913 | HCID 178516913 | — |
Reaction Steps
Using thianaphthene (5 mmol), [trans-4-(methoxy-methyl-carbamoyl)-cyclohexyl]-carbamic acid tert-butyl ester (2.5 mmol) and 3-oxo-3,4-dihydro-2H-benzo[1,4]thiazine-6-carbaldehyde (0.4 mmol) according to the same protocol as that described for example 1, steps 1.a to 1.c, the title compound was obtained as a yellowish solid (35 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07981886B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-fb19eaa3a7bd4d7d8953a2942a270bff |
| Source note | uspto-grants-2011_07 |