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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1012930Generated: October 31, 2026

Benzo(B)Thiophene → HCID 178516858, compound

https://huagongshe.com/reaction/1012930

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzo(B)ThiopheneHCID 7221—
Reactant3-oxo-3,4-dihydro-2H-1,4-benzoxazine-6-carbaldehydeHCID 10773638—
ReactantHCID 178502731HCID 178502731—
ProductHCID 178516858HCID 178516858—

Reaction Steps

The title compound was prepared according to the same protocol as that described for example 1, steps 1.a to 1.c, starting from thianaphthene (5 mmol), [trans-4-(methoxy-methyl-carbamoyl)-cyclohexyl]-carbamic acid tert-butyl ester (2.5 mmol) and 3-oxo-3,4-dihydro-2H-benzo[1,4]oxazine-6-carbaldehyde (0.4 mmol). A colourless solid (44 mg) was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07981886B2
Source datasetuspto-grants-2011_07
ORD IDord-213e38fd84ac4d209f58806cd302badf
Source noteuspto-grants-2011_07