HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Bromoethoxy)-4-chlorobenzene → (5-Chloro-3-{3-[2-(4-chloro-phenoxy)-ethyl]-4-oxo-3,4-dihydro-phthalazin-1-yl}-2-methyl-indol-1-yl)-acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Bromoethoxy)-4-chlorobenzene | HCID 74854 | — |
| Reactant | tert-butyl 2-(5-chloro-3-(4-hydroxyphthalazin-1-yl)-2-methyl-1H-indol-1-yl)acetate | HCID 58247168 | — |
| Product | (5-Chloro-3-{3-[2-(4-chloro-phenoxy)-ethyl]-4-oxo-3,4-dihydro-phthalazin-1-yl}-2-methyl-indol-1-yl)-acetic acid | HCID 59753850 | — |
Reaction Steps
The title compound was prepared from the product of example 16, step c) and 1-(2-bromo-ethoxy)-4-chloro-benzene using the procedure described in example 14. MS: ESI (negative): 520, 522 (M−H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07981912B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-f060dc9412504319a6896b21669d5c5a |
| Source note | uspto-grants-2011_07 |