Water → Ethyl 3-(3-(naphthalen-1-ylthio)propyl)-1h-indole-2-carboxylate

関与物質

反応手順

A mixture of EXAMPLE 10A (42 mg), naphthalene thiol (45 mg), and potassium carbonate (36 mg) in acetonitrile (2 mL) was heated at 80° C. for 3 days. The reaction mixture was poured into water, extracted with dichloromethane and purified by flash chromatography on silica gel with 0-20% ethyl acetate in hexanes.

情報源と証拠