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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1013306Generated: October 31, 2026

Cesium carbonate → HCID 67316412, compound

https://huagongshe.com/reaction/1013306

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCesium carbonateHCID 10796—
Reactant1-(3-Bromopropoxy)naphthaleneHCID 12959381—
ReactantHCID 67315809HCID 67315809—
SolventDimethylformamideHCID 6228—
SolventEthyl AcetateHCID 8857—
ProductHCID 67316412HCID 67316412—

Reaction Steps

To a solution of EXAMPLE 126B (1.14 g) and 1-(3-bromopropoxy)naphthalene (0.922 g) in N,N-dimethylformamide (20 ml) was added cesium carbonate (2.158 g). The reaction was stirred at room temperature overnight and diluted with ethyl acetate and washed with water. The organic layer was dried over sodium sulfate, filtered and concentrated. The residue was purified by flash chromatography, eluting with 0-50% dichloromethane in hexane to provide the title product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07981888B2
Source datasetuspto-grants-2011_07
ORD IDord-6d1543d3bfd145b88b7cfa47d103ddbb
Source noteuspto-grants-2011_07