HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium hydroxide, monohydrate → HCID 57951454, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium hydroxide, monohydrate | HCID 168937 | — |
| Reactant | HCID 57951458 | HCID 57951458 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 57951454 | HCID 57951454 | — |
Reaction Steps
A mixture of 3-methyl-1-oxa-2-azaspiro[4.5]dec-2-ene-8-carboxylic acid ethyl ester (570 mg, 2.5 mmol) in MeOH (15 ml) and lithium hydroxide monohydrate (284 mg, 3.8 mmol) in H2O (3 ml) was stirred overnight at RT.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07981883B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-a0cbc9a302744e57999502d069162383 |
| Source note | uspto-grants-2011_07 |