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HRID1014083

反应详情

EQUATION

反应方程式

HRID 1014083 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)Oc1ccccc1
HCID15891

Phenyl carbonochloridate

C7H5ClO2

结构：CC(C)CCNC(=O)c1ccccc1-c1ccccc1CN
HCID67316109

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)CCNC(=O)c1ccccc1-c1ccccc1CNC(=O)Oc1ccccc1
HCID9931732

未命名化合物

PROCEDURE

实验过程

From 0.34 mmol of 2′-aminomethylbiphenyl-2-carboxylic acid ( 3-methylbutyl)amide (precursor 5 c) and phenyl chloroformate, according to the general working procedure followed by extraction with EA and purification by flash chromatography 55 mg of 2′-(phenoxycarbonylaminomethyl)biphenyl-2-carboxylic acid (3-methylbutyl)amide were obtained as a resin. MS (ES+): m/e=417 (M+1).

WORKUP

后处理

  1. extractionfollowed by extraction with EA and purification by flash chromatography 55 mg of 2′-(phenoxycarbonylaminomethyl)biphenyl-2-carboxylic acid (3-methylbutyl)amide
  2. customwere obtained as a resin