HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Dimethylpropyl carbonochloridate → HCID 9955140, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Dimethylpropyl carbonochloridate | HCID 3352185 | — |
| Reactant | 2'-(Aminomethyl)-N-(2-phenylethyl)[1,1'-biphenyl]-2-carboxamide | HCID 15509384 | — |
| Product | HCID 9955140 | HCID 9955140 | — |
Reaction Steps
From 0.45 mmol of 2′-aminomethylbiphenyl-2-carboxylic acid phenethylamide (precursor 5 a) and neopentyl chloroformate, according to the general working procedure followed by extraction with EA and purification by flash chromatography 156 mg of 2′-(2,2-dimethylpropoxycarbonylaminomethyl)biphenyl-2-carboxylic acid phenethylamide were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07982045B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-abaa3f96dbc24e008c9be2db21f5aea0 |
| Source note | uspto-grants-2011_07 |