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HRID1014085

反应详情

EQUATION

反应方程式

HRID 1014085 的结构方程式

REACTANTS

反应物

2
结构：CC(C)S(=O)(=O)Cl
HCID82408

Isopropyl sulfonyl chloride

C3H7ClO2S

结构：CC(C)CCNC(=O)c1ccccc1-c1ccccc1CN
HCID67316109

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)CCNC(=O)c1ccccc1-c1ccccc1CNS(=O)(=O)C(C)C
HCID9887383

未命名化合物

PROCEDURE

实验过程

From 0.34 mmol of 2′-aminomethylbiphenyl-2-carboxylic acid (3-methylbutyl)amide (precursor 5 c) and isopropylsulfonyl chloride, according to the general working procedure followed by purification by flash chromatography 16 mg of 2′-(isopropylsulfonylaminomethyl)biphenyl-2-carboxylic acid (3-methylbutyl)amide were obtained as an oil. MS (ES+): m/e=403 (M+1).

WORKUP

后处理

  1. customfollowed by purification by flash chromatography 16 mg of 2′-(isopropylsulfonylaminomethyl)biphenyl-2-carboxylic acid (3-methylbutyl)amide
  2. customwere obtained as an oil