Acetone → HCID 67316339, compound

Participants

Reaction Conditions

Reaction Steps

To acetone (300 mL) was added 3-(3-methyl-4-nitrophenyl)pyridine (Intermediate B9, 20.25 g, 88.0 mmol)) and allyl bromide (42.6 g, 352.2 mmol, Aldrich), and the reaction was stirred at 60° C. for 12 h. Filtration removed the liquids and washing with MeOH (2×20 mL) afforded 3-[3-(methyloxy)-4-nitrophenyl]-1-(2-propen-1-yl)pyridinium bromide as a yellow solid (30.8 g, 99% yield).

Provenance & Evidence