HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 67317069, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | HCID 17603797 | HCID 17603797 | — |
| Product | HCID 67317069 | HCID 67317069 | — |
Reaction Steps
Addition of acetonitrile to 3-phenethoxybenzaldehyde gave 3-hydroxy-3-(3-phenethoxyphenyl)propanenitrile as a yellow oil. Yield (0.80 g, 80%): 1H NMR (400 MHz, CDCl3) δ 7.23-7.38 (m, 6H), 6.93-6.97 (m, 2H), 6.88 (dd, J=7.6, 1.8 Hz, 1H), 5.00 (t, J=″6.0 Hz, 1H), 4.18 (t, J=7.2 Hz, 2H), 3.12 (t, J=7.2 Hz, 2H), 2.75 (d, J=6.4 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07982071B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-337bb1046e78442a9afb11830b0c42c0 |
| Source note | uspto-grants-2011_07 |