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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1014658생성일: 2026년 10월 25일

1,3-Benzenediol, 4-methyl- → 5-(Cyclohexylmethoxy)-2-methylphenol

https://huagongshe.com/reaction/1014658

반응식

참여 물질

역할이름HCID투입량
반응물1,3-Benzenediol, 4-methyl-HCID 10333—
반응물Cyclohexane, (bromomethyl)-HCID 137636—
생성물5-(Cyclohexylmethoxy)-2-methylphenolHCID 67316675—

반응 단계

Alkylation of 4-methylbenzene-1,3-diol using (bromomethyl)cyclohexane following the method used in Example 154 gave 5-(cyclohexylmethoxy)-2-methylphenol as a light yellow oil. Yield (0.15 g, 8.5%): 1H NMR (400 MHz, CDCl3) δ 6.96 (d, J=8.4 Hz, 1H), 6.36-6.41 (m, 2H), 3.68 (d, J=6.4 Hz, 2H), 2.16 (s, 3H), 1.64-1.89 (m, 6H), 1.14-1.34 (m, 3H), 0.96-1.08 (m, 2H).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07982071B2
출처 데이터셋uspto-grants-2011_07
ORD IDord-0233f0f6facc4488a9e7adaa4261b760
출처 메모uspto-grants-2011_07