HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 59949122, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 15172765 | HCID 15172765 | — |
| Product | HCID 59949122 | HCID 59949122 | 46% |
Reaction Steps
This reaction is performed as previously described by Deechongkit, S.; You, S.-L.; Kelly, J. W. Org. Lett. 2004, 6, 497, using (R)-3-benzylsulfanyl-2-hydroxy-propionic acid methyl ester 2 and lithium hydroxide. (R)-3-Benzylsulfanyl-2-hydroxy-propionic acid 3 (3.08 g, 14.51 mmol, 46%) is isolated as a viscous oil: MS calculated for C10H12O3S (M+Na+) 235.1, found 235.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07985749B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-6fefe7afd24e40f4992f31b8328184a5 |
| Source note | uspto-grants-2011_07 |