1-(2-Nitroethenyl)-2-(trifluoromethyl)benzene → 2-(Trifluoromethyl)phenethylamine

HRID 1015004Notes

Reaction equation

HRID 1015004 reaction equation
[N+:1]([CH:4]=[CH:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[C:12]([F:15])([F:14])[F:13])([O-])=O.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[F:13][C:12]([F:14])([F:15])[C:7]1[CH:8]=[CH:9][CH:10]=[CH:11][C:6]=1[CH2:5][CH2:4][NH2:1]

Participants

3

Reactant 2

HCID 6882351-(2-Nitroethenyl)-2-(trifluoromethyl)benzeneHCID 21226445Aluminium lithium hydride

Product 1

HCID 698832-(Trifluoromethyl)phenethylamine

Procedure

In close analogy to the procedure described above, 1-(2-Nitro-vinyl)-2-trifluoromethyl-benzene is reacted with lithium aluminium hydride to provide the title compound.

Sources & evidence

ORD record
ord-01fb3c1d7452480faebb32fdfb5a191d
Source dataset
uspto-grants-2011_07
Patent number
US07985753B2

Reaction notes

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