Acetic Anhydride → N-[2-(4-Methylphenyl)ethyl]ethanimidic acid

HRID 1015010Notes

Reaction equation

[C:1]1([CH3:10])[CH:6]=[CH:5][C:4]([CH2:7][CH2:8][NH2:9])=[CH:3][CH:2]=1.[C:11](OC(=O)C)(=[O:13])[CH3:12]>>[C:1]1([CH3:10])[CH:6]=[CH:5][C:4]([CH2:7][CH2:8][NH:9][C:11](=[O:13])[CH3:12])=[CH:3][CH:2]=1

Participants

Reactant 2

HCID 7918Acetic Anhydride

HCID 76751p-Methylphenethylamine

Product 1

HCID 12441928N-[2-(4-Methylphenyl)ethyl]ethanimidic acid

Procedure

In close analogy to the procedure described above, 2-p-tolyl-ethylamine is reacted with acetic anhydride to provide the title compound.

Sources & evidence

ORD record: ord-b3607535763d481d82f6951f23d7cc31
Source dataset: uspto-grants-2011_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07985753B2

Reaction notes

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