Phosphorus oxide (P4O10) → HCID 15208262, compound

HRID 1015028Notes

Reaction equation

HRID 1015028 reaction equation
[C:1]1([CH3:13])[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[CH2:7][CH2:8][NH:9][C:10](=O)[CH3:11].O=P12OP3(OP(OP(O3)(O1)=O)(=O)O2)=O>>[CH3:11][C:10]1[C:3]2[C:2](=[C:1]([CH3:13])[CH:6]=[CH:5][CH:4]=2)[CH2:7][CH2:8][N:9]=1

Participants

3

Reactant 2

HCID 14812Phosphorus oxide (P4O10)HCID 15208261HCID 15208261, compound

Product 1

HCID 15208262HCID 15208262, compoundYield 59%

Procedure

In close analogy to the procedure described above, N-(2-o-tolyl-ethyl)-acetamide is reacted with phosphorus pentoxide to provide the title compound.

Sources & evidence

ORD record
ord-1b0136928caf47bd8e8df5960559abbe
Source dataset
uspto-grants-2011_07
Patent number
US07985753B2

Reaction notes

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