Phosphorus oxide (P4O10) → HCID 58416302, compound
Reaction equation
[O:1]1[C:6]2[CH:7]=[CH:8][CH:9]=[C:10]([CH2:11][CH2:12][NH:13][C:14](=O)[CH3:15])[C:5]=2[O:4][CH2:3][CH2:2]1.O=P12OP3(OP(OP(O3)(O1)=O)(=O)O2)=O>>[CH3:15][C:14]1[C:9]2[C:10](=[C:5]3[C:6](=[CH:7][CH:8]=2)[O:1][CH2:2][CH2:3][O:4]3)[CH2:11][CH2:12][N:13]=1Participants
3
Procedure
In close analogy to the procedure described above, N-[2-(2,3-dihydro-benzo[1,4]dioxin-5-yl)-ethyl]-acetamide is reacted with phosphorus pentoxide to provide the title compound.
Sources & evidence
- ORD record
- ord-bbbdd3848718487187ea42fa106f4cb3
- Source dataset
- uspto-grants-2011_07
- Patent number
- US07985753B2
Reaction notes
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