Iodide Ion → HCID 67300712, compound

HRID 1015463Notes

Reaction equation

HRID 1015463 reaction equation
OC[CH2:3][CH2:4][CH2:5][C:6]1[S:10][C:9]([C:11]([O:13][CH3:14])=[O:12])=[CH:8][CH:7]=1.[I-:15]>>[I:15][CH2:3][CH2:4][CH2:5][C:6]1[S:10][C:9]([C:11]([O:13][CH3:14])=[O:12])=[CH:8][CH:7]=1

Participants

3

Reactant 2

HCID 30165Iodide IonHCID 14796144Methyl 5-(4-hydroxybutyl)thiophene-2-carboxylate

Product 1

HCID 67300712HCID 67300712, compound

Procedure

Methyl 5-(4-hydroxybutyl)thiophene-2-carboxylate 112 (1.07 g, 4.99 mmol) was converted to 1.61 g (99%) iodide 113 according to the procedures described in Example 5.

Sources & evidence

ORD record
ord-5ef6b3c404d84eebb3976d708c28daa2
Source dataset
uspto-grants-2011_07
Patent number
US07985767B2

Reaction notes

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