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HRID1015940

反应详情

EQUATION

反应方程式

HRID 1015940 的结构方程式

REACTANTS

反应物

2
结构：C=C[C@@H]1C[C@]1(NC(=O)OC(C)(C)C)C(=O)OC
HCID10421813

Methyl (1R,2S)-1-[(tert-butoxycarbonyl)amino]-2-ethenylcyclopropane-1-carboxylate

C12H19NO4

结构：ClCCl.O=C(O)C(F)(F)F
HCID21863450

未命名化合物

PRODUCTS

生成物

1
结构：C=C[C@@H]1C[C@]1(N)C(=O)OC.O=C(O)C(F)(F)F
HCID67246036

未命名化合物

PROCEDURE

实验过程

N-Boc-(1R,2S)-1-amino-2-vinylcyclopropane carboxylic acid methyl ester (125 mg, 0.52 mmol) stirred in CH2Cl2/TFA (1:1, 2 mL) at RT for 90 minutes. Solvents removed under vacuum to yield (1R,2S)-1-amino-2-vinylcyclopropane carboxylic acid methyl ester trifluoroacetic acid salt.

WORKUP

后处理

  1. customSolvents removed under vacuum