HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Benzamido-3-methylbut-2-enoic acid → HCID 57889868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Benzamido-3-methylbut-2-enoic acid | HCID 55843 | — |
| Reactant | 4-(4-chlorophenyl)piperidine Hydrochloride | HCID 2757843 | — |
| Product | HCID 57889868 | HCID 57889868 | — |
Reaction Steps
The crude 2-benzamido-3-methylbut-2-enoic acid from Step 1 was coupled with 4-(4-chlorophenyl)piperidine hydrochloride in a similar manner as described for the preparation of Example 75 to provide Example 288, N-(1-(4-(4-chlorophenyl)piperidin-1-yl)-3-methyl-1-oxobut-2-en-2-yl)benzamide. MS found: 397 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07985861B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-40b6a95486104164a3d84c9efb02ba4a |
| Source note | uspto-grants-2011_07 |