反应详情

48.2 g of 5-(4-ethoxy-2,3-difluorophenyl)-2-pentyl-cyclohexanol were dissolved in 600 ml of dichloromethane, and 30 g of Celite were added. 35.6 g of pyridinium chlorochromate were added with stirring, and the mixture was stirred at RT overnight. Conventional work-up gave 5-(4-ethoxy-2,3-difluorophenyl)-2-pentyl-cyclohexanone.

1. addition30 g of Celite were added
2. stirringthe mixture was stirred at RT overnight