Bromine → HCID 11265458, compound

Participants

Reaction Conditions

Reaction Steps

Bromine (28.8 g, 0.18 mol) (dissolved in dioxane (500 ml)) was added dropwise to a solution of 2-methoxy-6-methylsulfanylbenzaldehyde (22 g, 0.12 mol) in dioxane (500 ml), and the mixture was stirred at 50° C. for 6 h. The mixture was then concentrated, the residue was taken up in CH2Cl2, and the mixture was washed with H2O , dried over MgSO4 and concentrated. The solid was recrystallized from diisopropyl ether.

Provenance & Evidence