3-Bromo-1-propanol → HCID 17798126, compound

HRID 1016321Notes

Reaction equation

HRID 1016321 reaction equation
[Br:1][C:2]1[CH:15]=[CH:14][C:13]2[S:12][C:11]3[C:6]4=[C:7]([C:17](=[O:20])[CH:18]=[CH:19][N:5]4[C:4]=2[CH:3]=1)[CH:8]=[C:9]([OH:16])[CH:10]=3.Br[CH2:22][CH2:23][CH2:24][OH:25]>>[Br:1][C:2]1[CH:15]=[CH:14][C:13]2[S:12][C:11]3[C:6]4=[C:7]([C:17](=[O:20])[CH:18]=[CH:19][N:5]4[C:4]=2[CH:3]=1)[CH:8]=[C:9]([O:16][CH2:22][CH2:23][CH2:24][OH:25])[CH:10]=3

Participants

3

Reactant 2

HCID 123083-Bromo-1-propanolHCID 18406549HCID 18406549, compound

Product 1

HCID 17798126HCID 17798126, compoundYield 36%

Procedure

According to Example 34, the compound (145 mg) produced in Example 58 was reacted with 3-bromopropanol (65 μl) to obtain the title compound (62 mg; 36%).

Sources & evidence

ORD record
ord-1ccb214d50d547119e71e25d02771890
Source dataset
uspto-grants-2002_11
Patent number
US06476021B1

Reaction notes

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