HuagongsheHuagongshe Chemistry Print Report · For research reference only
DL-alanine → HCID 11401639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | DL-alanine | HCID 602 | — |
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Octanoyl chloride | HCID 8124 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Product | HCID 11401639 | HCID 11401639 | — |
Reaction Steps
The preparation is carried out analogously to the procedure of Example 4A using 16.5 g (0.185 mol) of D,L-alanine, 41.23 g (0.407 mol) of triethylamine, 44.27 g (0.407 mol) of trimethylsilyl chloride and 30.12 g (0.185 mol) of octanoyl chloride. The product crystallizes from toluene/n-hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06476029B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-d253c6d56a3b46e8a14e7f2620a62ec8 |
| Source note | uspto-grants-2002_11 |