Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178420581 | HCID 178420581 | — |
| Product | HCID 178467551 | HCID 178467551 | — |
Reaction Steps
Bis(cyclopentadienyl)ruthenium (3 g), acetic anhydride (10 ml), and 85% phosphoric acid (2.0 ml) were placed in a round-bottom flask, and the mixture was heated at 85° C. for one hour. The formed reaction product was neutralized by use of sodium hydroxide, recrystallized, and subjected to extraction by use of hexane, thereby yielding 1.8 g of (acetylcyclopentadienyl)cyclopentadienylruthenium.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06476247B1 |
|---|
| Source dataset | uspto-grants-2002_11 |
|---|
| ORD ID | ord-2ded447ace29464097ac35218155c5f7 |
|---|
| Source note | uspto-grants-2002_11 |
|---|
