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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1016715Generated: October 25, 2026

Benzaldehyde → HCID 10443568, compound

https://huagongshe.com/reaction/1016715

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzaldehydeHCID 240—
ReactantMethanolHCID 887—
Reactant2-AminoheptaneHCID 5603—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
ProductHCID 10443568HCID 10443568—

Reaction Steps

100 ml of methanol and 100 mmol of 2-heptylamine are initially taken and 100 mmol of benzaldehyde are added dropwise at 24° C. in the course of 15 minutes. Stirring is effected for 6 hours at 24° C., the completeness of the iminization is checked by GC, 0.5 g of Pd/C (10% by weight) is added and the crude mixture is hydrogenated with hydrogen for 5 hours at atmospheric pressure. A sample is taken and the composition is investigated by GC analysis.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06476268B1
Source datasetuspto-grants-2002_11
ORD IDord-ba1edca4717347c4aa02c2f111f30d6f
Source noteuspto-grants-2002_11