Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 3,4-Diethoxybenzaldehyde | HCID 74847 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 22039301 | HCID 22039301 | — |
Reaction Steps
2.13 ml of fuming nitric acid were added within 30 minutes to a solution, cooled to −30° C. of 10 g of 3,4-diethoxybenzaldehyde in 185 ml of 1,2-dichloroethane. Subsequently, the reaction mixture was left to warm to 0° C. and was poured on to ice. The product was isolated by extraction. There were obtained 12.06 g of 4,5-diethoxy-2-nitro-benzaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06476264B2 |
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| Source dataset | uspto-grants-2002_11 |
|---|
| ORD ID | ord-ed09a2801a384f6b9ec12b5e2e147cb5 |
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| Source note | uspto-grants-2002_11 |
|---|
