HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorophenylacetic acid → 2-[(3-Fluorophenyl)acetamido]butyric acid isobutyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorophenylacetic acid | HCID 67617 | — |
| Reactant | Isobutyl 2-aminobutyrate | HCID 13743360 | — |
| Product | 2-[(3-Fluorophenyl)acetamido]butyric acid isobutyl ester | HCID 54019925 | — |
Reaction Steps
Following General Procedure I′ above and using 3-fluorophenylacetic acid (Aldrich) and iso-butyl 2-aminobutyrate (prepared following General Procedure J′ above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06476263B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-e49a3f146fcf4f6dba4896c4baab4806 |
| Source note | uspto-grants-2002_11 |