HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Bromophenyl)acetic acid → 2-[(3-bromophenyl)acetamido]butyric Acid isobutyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Bromophenyl)acetic acid | HCID 74653 | — |
| Reactant | Isobutyl 2-aminobutyrate | HCID 13743360 | — |
| Product | 2-[(3-bromophenyl)acetamido]butyric Acid isobutyl Ester | HCID 15481771 | — |
Reaction Steps
Following General Procedure I′ above and using 3-bromophenylacetic acid (Aldrich) and iso-butyl 2-aminobutyrate (prepared following General Procedure J′ above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure. NMR data was as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06476263B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-4711a27e76ea4e2bb6a26b47bf5ea7c2 |
| Source note | uspto-grants-2002_11 |