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HRID1016921

反应详情

EQUATION

反应方程式

HRID 1016921 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)CN.Cl
HCID2723640

Ethyl glycinate hydrochloride

C4H10ClNO2

结构：C[C@H](NC(=O)Cc1cccc([N+](=O)[O-])c1)C(=O)O
HCID53788870

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)CNC(=O)[C@H](C)NC(=O)Cc1cccc([N+](=O)[O-])c1
HCID9819161

未命名化合物

PROCEDURE

实验过程

Following General Procedure C and using N-(3-nitrophenylacetyl)-L-alanine (prepared from 3-nitrophenylacetic acid (Aldrich) and L-alanine ethyl ester hydrochloride (Sigma) using General Procedure C, followed by hydrolysis using General Procedure AF) and glycine ethyl ester hydrochloride (Sigma), the title compound was prepared as a solid (mp=164-165 ° C.). The product was purified by silica gel chromatography using EtOAc as the eluent, followed by recrystallization from EtOAc.

WORKUP

后处理

  1. customThe product was purified by silica gel chromatography
  2. customfollowed by recrystallization from EtOAc