HuagongsheHuagongshe Chemistry Print Report · For research reference only
(-)-2-Aminobutyric acid → Methyl N-[N-(3-nitrophenylacetyl)-L-alaninyl]-(S)-2-aminobutanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (-)-2-Aminobutyric acid | HCID 80283 | — |
| Reactant | N-(3-Nitrophenylacetyl)-L-alanine | HCID 53788870 | — |
| Reactant | (S)-methyl 2-aminobutanoate hydrochloride | HCID 71313169 | — |
| Product | Methyl N-[N-(3-nitrophenylacetyl)-L-alaninyl]-(S)-2-aminobutanoate | HCID 22894965 | — |
Reaction Steps
Following General Procedure C and using N-(3-nitrophenylacetyl)-L-alanine (from Example D11 above) and methyl (S)-2-aminobutanoate hydrochloride prepared from (S)-(+)-2-aminobutyric acid (Aldrich) using General Procedure H), the title compound was prepared as a solid (mp=154-157° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06476263B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-4c2f1790e37e4ed1a06e4fa1bfe200a0 |
| Source note | uspto-grants-2002_11 |