HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(Phenylacetyl)-L-alanine → N-[N-(Phenylacetyl)-L-alaninyl]-L-isoleucine Methyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(Phenylacetyl)-L-alanine | HCID 7004640 | — |
| Reactant | Isoleucine methyl ester hydrochloride | HCID 11171351 | — |
| Product | N-[N-(Phenylacetyl)-L-alaninyl]-L-isoleucine Methyl Ester | HCID 22895048 | — |
Reaction Steps
Following General Procedure A and using N-(phenylacetyl)-L-alanine (from Example B1 above) and L-isoleucine methyl ester hydrochloride (Sigma), the title compound was prepared. The reaction was monitored by tlc (Rf=0.24 in 50% EtOAc/hexanes).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06476263B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-db1ab4e3f43c4ad2b6c34eb482f3974c |
| Source note | uspto-grants-2002_11 |