HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl valinate hydrochloride → HCID 22895053, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl valinate hydrochloride | HCID 111190 | — |
| Reactant | N-(Phenylacetyl)-L-alanine | HCID 7004640 | — |
| Product | HCID 22895053 | HCID 22895053 | — |
Reaction Steps
Following General Procedure A and using N-(phenylacetyl)-L-alanine (fromo Example B1 above) and L-valine methyl ester hydrochloride (Aldrich), the title compound was prepared as a solid (mp=112-115° C.). The reaction was monitored by tlc (Rf=0.33 in 50% EtOAc/hexanes) and the product was not purified.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06476263B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-6de7db779d3e44bb8e1865c4f2a2223f |
| Source note | uspto-grants-2002_11 |