HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(Phenylacetyl)-L-alanine → HCID 22894968, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(Phenylacetyl)-L-alanine | HCID 7004640 | — |
| Reactant | methyl (2S)-2-aminopentanoate hydrochloride | HCID 14118488 | — |
| Product | HCID 22894968 | HCID 22894968 | — |
Reaction Steps
Following General Procedure A and using N-(phenylacetyl)-L-alanine (from Example B1 above) and methyl 2-(S)-aminopentanoate hydrochloride (prepared from L-2-aminovaleric acid (Bachem) using General Procedure H (without extractions)), the title compound was prepared as a solid (mp=135-137° C.). The reaction was monitored by tlc (Rf=0.30 in 50% EtOAc/hexanes).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06476263B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-d159bf89ce8d4032a987ae5c7b752728 |
| Source note | uspto-grants-2002_11 |