HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dimethoxybenzaldehyde → 2-(2,3-dimethoxyphenyl)-3H-quinazolin-4-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dimethoxybenzaldehyde | HCID 66581 | — |
| Reactant | 2-(2-methoxyphenyl)-3H-quinazolin-4-one | HCID 135436005 | — |
| Product | 2-(2,3-dimethoxyphenyl)-3H-quinazolin-4-one | HCID 135489849 | 86% |
Reaction Steps
According to the preparation of 42, 2,3-dimethoxybenzaldehyde (36) (1.2 g, 7.3 mmol) was used to afford 45 (1.8 g, 86.0%) as pale yellow needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06479499B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-c7f9fc1d0619479c85701732b639016a |
| Source note | uspto-grants-2002_11 |