HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxybenzaldehyde → 6-(3-methoxyphenyl)-7H-[1,3]dioxolo[4,5-g]quinazolin-8-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxybenzaldehyde | HCID 11569 | — |
| Reactant | 6-Aminobenzo[D][1,3]dioxole-5-carboxamide | HCID 10726053 | — |
| Reactant | 2-(2-methoxyphenyl)-3H-quinazolin-4-one | HCID 135436005 | — |
| Product | 6-(3-methoxyphenyl)-7H-[1,3]dioxolo[4,5-g]quinazolin-8-one | HCID 135511101 | 8.8% |
Reaction Steps
According to the preparation of 42, 16 (1.0 g, 5.5 mmol) and 3-methoxybenzaldehyde (34) (0.7 g, 5.5 mmol) were used to afford 54 (0.1 g, 8.8%) as pale yellow needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06479499B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-6a306b9813ee4e3eb0d56078bb324aed |
| Source note | uspto-grants-2002_11 |